Diagnostic Summary Reference Card

Module 02 — Contamination & Gas Loads | VacTech, Selkirk College

Five Gas Load Sources

💨

Outgassing

Gas molecules desorbing from chamber walls and internal surfaces. Dominant below ~1 mbar. Decays with time (approximately as t−1). Reduced by bakeout and surface cleaning.

💧

Permeation

Atmospheric gas diffusing through solid materials (especially elastomer seals). Small, constant rate. Cannot be eliminated — only reduced by material selection (e.g., Viton over Buna-N).

Real Leak

Gas entering through a physical gap — damaged O-ring, loose fitting, cracked weld. Produces a constant, linear pressure rise in rate-of-rise tests. Detectable by helium leak testing.

🕳

Virtual Leak

Trapped gas escaping slowly from blind holes, O-ring grooves, or double seals. Looks like a leak but has no external path. Produces a decaying rate-of-rise (gas reservoir empties). Fix: vent holes, proper groove design.

Backstreaming

Pump oil vapour migrating into the chamber against the pumping direction. Significant with oil-sealed rotary vane pumps at low pressures. Mitigated by foreline traps or oil-free pumps (scroll, diaphragm).

Rate-of-Rise Test Interpretation

Pattern Curve Shape Diagnosis Action
Linear rise P ╱╱╱ (constant slope) Real leak — constant gas inflow from outside Leak-check all seals, fittings, welds. Use helium spray method.
Decaying rise P ╱‾‾ (fast then slow) Outgassing — surface desorption decreasing over time Extended pump time or mild bakeout (60–120 °C). Clean surfaces with IPA.
Plateau + decay P ╱‾─ (rise, level, slow decay) Virtual leak — trapped volume releasing finite gas reserve Inspect for blind holes, double seals, trapped volumes. Add vent grooves.
No rise P ─── (flat) System is tight — gas load below detection threshold System passes. Proceed with process.

Contamination Indicators Checklist